© Journal Of Chemical Society Of Nigeria (jcsn) . 2010. Vol. 35 No. 1
Publisher: Chemical Society of Nigeria
Synthesis of Novel Fused Tris-1,2,3-Triazoles From Melamine
O. J. Abayeh, N. U. Ibok
KEYWORDS: melamine, fused tris-azo dyes, cyclisation, 1,2,3-triazoles, DMF
ABSTRACT:The Synthesis of relatively unknown fused tris-1.2.3-triazoles [2a-e] from melamine is reported. This was achieved via the oxidative cyclization of tris-azo dyes [la-e] in DMF and dry air. The compounds [2a-e] were obtained in low to moderate yields (27.41-66.23%). The spectral data, IR, 1Hnmr and 13Cnmr agree with the assigned structures.
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